Author: Josh Winans
Josh is a postdoc in the McGrath lab working on disruptive membrane technologies.

Hydraulic permeability of SiN-NP wafer #'s 1029 and 1030 with "clean" water

Sarah, Tejas, and I bought some “Invitrogen Ultrapure DI water” from the medical center to see if we would find a different permeability using the clean water vs the water from the Barnstead. Sarah and I repeated our permeability tests

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Updated: Continued Au separations with SiN-NP wafer #'s 1029 and 1030

Sarah and I did some more gold separations with 10, 20, 40, 50, 60, 80 and 100 nm Au particles.  We used the “clean” water purchased from the medical center.  Same as last time, we diluted the “as-bought” gold 3

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SiN NP wafer #'s 1029 and 1030 pore size revisions

Our work with permeance and hydraulic permeability tests on the SiN-NP seemed to show that the porosity and pore sizes I had calculated from the STEM images were too high.  I used URnano’s TEM to get better quality images and,

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50 nm thick pnc-Si on wafer # 760

I found another old wafer # 760 and asked Josh Miller to deposit a 25-50-25 OSO stack.  He did a standard RTP of 1050 C, 60 s, 100 C/s.  (and Josh Miller did the EDP etch, so this is really

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Au separations with SiN-NPs

Ultimately we want to use SiN-NP filters to separate viruses or some other biological species, but repeated attempts to pass 20 nm fluorospheres in water or PBS have failed.  Au particles, however, have passed through the filters.  This post reports

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Continued analysis of SiN-NP permeance and permeability

Following up on our previous work with SiN-NP with varied RIE times, Sarah and I measured permeability and permeance using a new measuring system better suited to the higher permeance and permeability we expect with the larger pores and higher porosity.

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pnc-Si removal from SiN-NP chips

JP and Josh Miller used the Xactic Si etcher to remove the pnc-Si from SiN-NP samples.  I believe they ran cycles until the samples looked visibly like SiN only.  Below are some SEM cross-sections showing before and after images of

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Gold NP separations with SiN-NP

Karl and attempted to pass 10, 20, 40 and 50 nm Au NPs through samples from the center of wafer # 1019 (avg por dia 50-60 nm, porosity ~27%).  The bottles of stock Au from BBI solutions do not have

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Fluorosphere separations with SiN-NP SEPCONS

Karl and I attempted once again to filter particles with the SiN-NP 5 slot SEPCON chips.  (wafer # 1019, 27% porosity, avg. pore dia. – 54 nm in the center, 30%, 61 nm at the perimeter, histograms below)   We

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SiN-NP with varied RIE times

We used 4″ wafers with 40 nm pnc-Si on 50 nm RV SiN (RTP 1050 C, 100 C/s, 60 s). JP ran a series of RIE times from 10 to 50 s with 10 s intervals.  (We had initially planned on

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